articleJournal of the American Chemical SocietyMar 6, 2015Closed access

Size-Dependent Electrocatalytic Reduction of CO 2 over Pd Nanoparticles

Chinese Academy of Sciences · Dalian Institute of Chemical Physics · +2 more institutions

PubMed
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Abstract

Size effect has been regularly utilized to tune the catalytic activity and selectivity of metal nanoparticles (NPs). Yet, there is a lack of understanding of the size effect in the electrocatalytic reduction of CO2, an important reaction that couples with intermittent renewable energy storage and carbon cycle utilization. We report here a prominent size-dependent activity/selectivity in the electrocatalytic reduction of CO2 over differently sized Pd NPs, ranging from 2.4 to 10.3 nm. The Faradaic efficiency for CO production varies from 5.8% at -0.89 V (vs reversible hydrogen electrode) over 10.3 nm NPs to 91.2% over 3.7 nm NPs, along with an 18.4-fold increase in current density. Based on the Gibbs free energy…

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