articleJournal of the American Chemical SocietyOct 20, 2014GREEN OA

Gold–Copper Nanoalloys Supported on TiO 2 as Photocatalysts for CO 2 Reduction by Water

Instituto de Tecnología Química · Universitat Politècnica de València

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Abstract

Commercial P25 modified by Au-Cu alloy nanoparticles as thin film exhibits, for CO2 reduction by water under sun simulated light, a rate of methane production above 2000 μmol (g of photocatalyst)(-1) h(-1). Although evolution of hydrogen is observed and O2 and ethane detected, the selectivity of conduction band electrons for methane formation is almost complete, about 97%. This photocatalytic behavior is completely different from that measured for Au/P25 (hydrogen evolution) and Cu/P25 (lower activity, but similar methane selectivity). Characterization by TEM, XPS, and UV-vis spectroscopy shows that Au and Cu are alloyed in the nanoparticles. FT-IR spectroscopy and chemical analysis have allowed one to detect…

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