articleThe Journal of Physical Chemistry BMay 13, 2004Closed access

Carbon-Supported Pt and PtRu Nanoparticles as Catalysts for a Direct Methanol Fuel Cell

National University of Singapore · Institute of Materials Research and Engineering

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Abstract

Nanosized Pt and PtRu colloids were prepared by a microwave-assisted polyol process and transferred to a toluene solution of decanthiol. Vulcan XC-72 was then added to the toluene solution to adsorb the thiolated Pt and PtRu colloids. TEM examinations showed nearly spherical particles and narrow size distributions for both supported and unsupported metals. The carbon-supported Pt and PtRu nanoparticles were activated by thermal treatment to remove the thiol stabilizing shell. All Pt and PtRu catalysts (except Pt23Ru77) showed the X-ray diffraction pattern of a face-centered cubic (fcc) crystal structure, whereas the Pt23Ru77 alloy was more typical of the hexagonal close-packed (hcp) structure. The…

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