articleJournal of the American Chemical SocietyJan 29, 2013Closed access

π-Conjugated Nickel Bis(dithiolene) Complex Nanosheet

The University of Tokyo · Nagoya University · +3 more institutions

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Abstract

A π-conjugated nanosheet comprising planar nickel bis(dithiolene) complexes was synthesized by a bottom-up method. A liquid-liquid interfacial reaction using benzenehexathiol in the organic phase and nickel(II) acetate in the aqueous phase produced a semiconducting bulk material with a thickness of several micrometers. Powder X-ray diffraction analysis revealed that the crystalline portion of the bulk material comprised a staggered stack of nanosheets. A single-layer nanosheet was successfully realized using a gas-liquid interfacial reaction. Atomic force microscopy and scanning tunneling microscopy confirmed that the π-conjugated nanosheet was single-layered. Modulation of the oxidation state of the nanosheet…

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Authors

11

Topics & keywords

Keywords
  • Nanosheet
  • Chemistry
  • Nickel
  • Conjugated system
  • Scanning tunneling microscope
  • Chemical engineering
  • Phase (matter)
  • Redox
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