articleAngewandte Chemie International EditionAug 4, 2016Closed access

Single Cobalt Atoms with Precise N‐Coordination as Superior Oxygen Reduction Reaction Catalysts

University of Science and Technology of China · Collaborative Innovation Center of Quantum Matter · +4 more institutions

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Abstract

A new strategy for achieving stable Co single atoms (SAs) on nitrogen-doped porous carbon with high metal loading over 4 wt % is reported. The strategy is based on a pyrolysis process of predesigned bimetallic Zn/Co metal-organic frameworks, during which Co can be reduced by carbonization of the organic linker and Zn is selectively evaporated away at high temperatures above 800 °C. The spherical aberration correction electron microscopy and extended X-ray absorption fine structure measurements both confirm the atomic dispersion of Co atoms stabilized by as-generated N-doped porous carbon. Surprisingly, the obtained Co-Nx single sites exhibit superior ORR performance with a half-wave potential (0.881 V) that is…

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