articleJournal of the American Chemical SocietyJul 11, 2017Closed access

Ammonia Electrosynthesis with High Selectivity under Ambient Conditions via a Li + Incorporation Strategy

South China University of Technology · Xiamen University

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Abstract

We report the discovery of a dramatically enhanced N2 electroreduction reaction (NRR) selectivity under ambient conditions via the Li+ incorporation into poly(N-ethyl-benzene-1,2,4,5-tetracarboxylic diimide) (PEBCD) as a catalyst. The detailed electrochemical evaluation and density functional theory calculations showed that Li+ association with the O atoms in the PEBCD matrix can retard the HER process and can facilitate the adsorption of N2 to afford a high potential scope for the NRR process to proceed in the “[O—Li+]·N2—Hx” alternating hydrogenation mode. This atomic-scale incorporation strategy provides new insight into the rational design of NRR catalysts with higher selectivity.

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613
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Authors

7

Topics & keywords

Keywords
  • Chemistry
  • Electrosynthesis
  • Selectivity
  • Ammonia
  • Inorganic chemistry
  • Nuclear chemistry
  • Organic chemistry
  • Electrochemistry
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