Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR
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Abstract
The field of dynamic nuclear polarization has undergone tremendous developments and diversification since its inception more than 6 decades ago. In this review we provide an in-depth overview of the relevant topics involved in DNP-enhanced MAS NMR spectroscopy. This includes the theoretical description of DNP mechanisms as well as of the polarization transfer pathways that can lead to a uniform or selective spreading of polarization between nuclear spins. Furthermore, we cover historical and state-of-the art aspects of dedicated instrumentation, polarizing agents, and optimization techniques for efficient MAS DNP. Finally, we present an extensive overview on applications in the fields of structural biology and…
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4Topics & keywords
Topics
Keywords
- Spins
- Polarization (electrochemistry)
- Hyperpolarization (physics)
- Solid-state nuclear magnetic resonance
- Nanotechnology
- Nuclear magnetic resonance spectroscopy
- Physics
- Materials science
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