articleJournal of the American Chemical SocietyOct 10, 2017Closed access

Exclusive Ni–N 4 Sites Realize Near-Unity CO Selectivity for Electrochemical CO 2 Reduction

University of Science and Technology of China · National Synchrotron Radiation Laboratory · +1 more institution

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Abstract

Electrochemical reduction of carbon dioxide (CO2) to value-added carbon products is a promising approach to reduce CO2 levels and mitigate the energy crisis. However, poor product selectivity is still a major obstacle to the development of CO2 reduction. Here we demonstrate exclusive Ni–N4 sites through a topo-chemical transformation strategy, bringing unprecedentedly high activity and selectivity for CO2 reduction. Topo-chemical transformation by carbon layer coating successfully ensures preservation of the Ni–N4 structure to a maximum extent and avoids the agglomeration of Ni atoms to particles, providing abundant active sites for the catalytic reaction. The Ni–N4 structure exhibits excellent activity for…

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