articleAngewandte Chemie International EditionJul 8, 2019Closed access

Switching on the Photocatalysis of Metal–Organic Frameworks by Engineering Structural Defects

University of Science and Technology of China · Hefei National Center for Physical Sciences at Nanoscale · +1 more institution

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Abstract

Abstract Defect engineering is a versatile approach to modulate band and electronic structures as well as materials performance. Herein, metal–organic frameworks (MOFs) featuring controlled structural defects, namely UiO‐66‐NH 2 ‐X (X represents the molar equivalents of the modulator, acetic acid, with respect to the linker in synthesis), were synthesized to systematically investigate the effect of structural defects on photocatalytic properties. Remarkably, structural defects in MOFs are able to switch on the photocatalysis. The photocatalytic H 2 production rate presents a volcano‐type trend with increasing structural defects, where Pt@UiO‐66‐NH 2 ‐100 exhibits the highest activity. Ultrafast transient…

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