articleAdvanced Functional MaterialsSep 2, 2019Closed access

3D Hierarchical ZnIn 2 S 4 Nanosheets with Rich Zn Vacancies Boosting Photocatalytic CO 2 Reduction

Jilin University · State Key Laboratory of Inorganic Synthesis and Preparative Chemistry · +1 more institution

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Abstract

Abstract Zinc vacancy (V Zn ) is successfully introduced into 3D hierarchical ZnIn 2 S 4 (3D‐ZIS). The photo‐electrochemical experiments demonstrate that the charge separation and carrier transfer are more efficient in the 3D‐ZIS with rich V Zn . Of note, for the first time, it is found that V Zn can decrease the carrier transport activation energy (CTAE), from 1.14 eV for Bulk‐ZIS (Bulk ZnIn 2 S 4 ) to 0.93 eV for 3D‐ZIS, which may provide a feasible platform for further understanding the mechanism of photocatalytic CO 2 reduction. In situ Fourier transform infrared (FT‐IR) results reveal that the presence of rich V Zn ensures CO 2 chemical activation, promoting single‐electron reduction of CO 2 to CO 2 − .…

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