articleNature CommunicationsSep 19, 2019GOLD OA

Regulating the coordination structure of single-atom Fe-NxCy catalytic sites for benzene oxidation

China University of Petroleum, East China · Tsinghua University · +5 more institutions

PubMed
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Abstract

Abstract Atomically dispersed metal-N-C structures are efficient active sites for catalyzing benzene oxidation reaction (BOR). However, the roles of N and C atoms are still unclear. We report a polymerization-regulated pyrolysis strategy for synthesizing single-atom Fe-based catalysts, and present a systematic study on the coordination effect of Fe-N x C y catalytic sites in BOR. The special coordination environment of single-atom Fe sites brings a surprising discovery: Fe atoms anchored by four-coordinating N atoms exhibit the highest BOR performance with benzene conversion of 78.4% and phenol selectivity of 100%. Upon replacing coordinated N atoms by one or two C atoms, the BOR activities decrease gradually.…

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