articleNano LettersFeb 1, 2022Closed access

Atomic Tuning of Single-Atom Fe–N–C Catalysts with Phosphorus for Robust Electrochemical CO 2 Reduction

University of Science and Technology of China · Hefei National Center for Physical Sciences at Nanoscale · +4 more institutions

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Abstract

The electrochemical reduction of CO2 to produce carbon-based fuels and chemicals possesses huge potentials to alleviate current environmental problems. However, it is confronted by great challenges in the design of active electrocatalysts with low overpotentials and high product selectivity. Here we report the atomic tuning of a single-Fe-atom catalyst with phosphorus (Fe–N/P–C) on commercial carbon black as a robust electrocatalyst for CO2 reduction. The Fe–N/P–C catalyst exhibits impressive performance in the electrochemical reduction of CO2 to CO, with a high Faradaic efficiency of 98% and a high mass-normalized turnover frequency of 508.8 h–1 at a low overpotential of 0.34 V. On the basis of ex-situ X-ray…

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