articleAdvanced MaterialsFeb 22, 2022Closed access

Cation‐Vacancy‐Enriched Nickel Phosphide for Efficient Electrosynthesis of Hydrogen Peroxides

The University of Sydney · University of Science and Technology of China · +3 more institutions

PubMed
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Abstract

Abstract Electrocatalytic hydrogen peroxide (H 2 O 2 ) synthesis via the two‐electron oxygen reduction reaction (2e ORR) pathway is becoming increasingly important due to the green production process. Here, cationic vacancies on nickel phosphide, as a proof‐of‐concept to regulate the catalyst's physicochemical properties, are introduced for efficient H 2 O 2 electrosynthesis. The as‐fabricated Ni cationic vacancies (V Ni )‐enriched Ni 2− x P‐V Ni electrocatalyst exhibits remarkable 2e ORR performance with H 2 O 2 molar fraction of >95% and Faradaic efficiencies of >90% in all pH conditions under a wide range of applied potentials. Impressively, the as‐created V Ni possesses superb long‐term durability…

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