articleJournal of the American Chemical SocietyAug 4, 2022Closed access

Role of Electronic Structure on Nitrate Reduction to Ammonium: A Periodic Journey

Oregon State University · Lawrence Berkeley National Laboratory · +2 more institutions

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Abstract

Electrocatalysis is a promising approach to convert waste nitrate to ammonia and help close the nitrogen cycle. This renewably powered ammonia production process sources hydrogen from water (as opposed to methane in the thermal Haber–Bosch process) but requires a delicate balance between a catalyst’s activity for the hydrogen evolution reaction (HER) and the nitrate reduction reaction (NO3RR), influencing the Faradaic efficiency (FE) and selectivity to ammonia/ammonium over other nitrogen-containing products. We measure ammonium FEs ranging from 3.6 ± 6.6% (on Ag) to 93.7 ± 0.9% (on Co) across a range of transition metals (TMs; Ti, Fe, Co, Ni, Ni0.68Cu0.32, Cu, and Ag) in buffered neutral media. To better…

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