articleJournal of the American Chemical SocietyMar 14, 2023Closed access

Hexagonal Cobalt Nanosheets for High-Performance Electrocatalytic NO Reduction to NH 3

Hunan University · State Key Laboratory of Chemobiosensing and Chemometrics · +2 more institutions

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Abstract

Electrocatalytic nitric oxide (NO) reduction not only provides an extremely promising strategy for ambient NH3 generation but also alleviates the artificially disrupted N-cycle balance. However, exploring efficient electrocatalysts to enhance the NO electroreduction performance remains a significant challenge. Herein, a hexagonal-close-packed Co nanosheet (hcp-Co) is prepared and exhibits a high NH3 yield of 439.50 μmol cm–2 h–1 and a Faraday efficiency of 72.58%, outperforming the face-centered cubic phase of the Co nanosheet (fcc-Co) and most reported electrocatalysts. Through the combination of density functional theory calculations and NO temperature-programmed desorption experiments, the superior…

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