articleAngewandte Chemie International EditionMay 8, 2023HYBRID OA

Solar Light Driven H 2 O 2 Production and Selective Oxidations Using a Covalent Organic Framework Photocatalyst Prepared by a Multicomponent Reaction

Technische Universität Berlin

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Abstract

Abstract A chemically stable 2D microporous COF ( PMCR‐1 ) was synthesized via the multicomponent Povarov reaction. PMCR‐1 exhibits a remarkable and long‐term stable photocatalytic H 2 O 2 production rate (60 h) from pure and sea water under visible light. The H 2 O 2 production is markedly enhanced when benzyl alcohol (BA) is added as reductant, which is also due to a strong π–π interaction of BA with dangling phenyl moieties in the COF pores introduced by the multicomponent Povarov reaction. Motivated by the concomitant BA oxidation to benzaldehyde during H 2 O 2 formation, the photocatalytic oxidation of various organic substrates such as benzyl amine and methyl sulfide derivatives was investigated. It is…

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190
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Authors

3

Topics & keywords

Keywords
  • Photocatalysis
  • Benzyl alcohol
  • Benzaldehyde
  • Microporous material
  • Photochemistry
  • Sulfide
  • Amine gas treating
  • Catalysis
UN Sustainable Development Goals
  • Life below water
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