articleJournal of the American Chemical SocietyJan 18, 2024GREEN OA

Water-Enhanced Direct Air Capture of Carbon Dioxide in Metal–Organic Frameworks

Kavli Energy NanoScience Institute · University of California, Berkeley · +2 more institutions

PubMed
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Abstract

We have developed two series of amine-functionalized zirconium (Zr) metal–organic framework-808 (MOF-808), which were produced by postsynthetic modifications to have either amino acids coordinated to Zr ions (MOF-808-AAs) or polyamines covalently bound to the chloro-functionalized structure (MOF-808-PAs). These MOF variants were comprehensively characterized by liquid-state 1H nuclear magnetic resonance (NMR) measurements and potentiometric acid–base titration to determine the amounts of amines, energy-dispersive X-ray spectroscopy to assess the extent of covalent substitution by polyamines, powder X-ray diffraction analysis to verify the maintenance of the MOF crystallinity and structure after postsynthetic…

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