articleACS Central ScienceFeb 20, 2024DIAMOND OA

Unraveling and Resolving the Inconsistencies in Tafel Analysis for Hydrogen Evolution Reactions

University of California, Los Angeles · California NanoSystems Institute

PubMed
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Abstract

The Tafel slope represents a critical kinetic parameter for mechanistic studies of electrochemical reactions, including the hydrogen evolution reaction (HER). Linear fitting of the polarization curve in a N2-saturated electrolyte is commonly used to determine Tafel slopes, which is, however, frequently plagued with inconsistencies. Our systematic studies reveal that the Tafel slopes derived from this approach are loading- and potential-dependent, and could substantially exceed the theoretical limits. Our analyses indicate that this discrepancy is largely attributed to the locally trapped HER-generated H2 in the catalyst layer. A non-negligible hydrogen oxidation reaction (HOR) current more prominently offsets…

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