articleAngewandte Chemie International EditionMar 1, 2024Closed access

Efficient Homolytic Cleavage of H 2 O 2 on Hydroxyl‐Enriched Spinel CuFe 2 O 4 with Dual Lewis Acid Sites

Guangzhou University · Nanchang Hangkong University

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Abstract

Abstract Traditional H 2 O 2 cleavage mediated by macroscopic electron transfer (MET) not only has low utilization of H 2 O 2 , but also sacrifices the stability of catalysts. We present a non‐redox hydroxyl‐enriched spinel (CuFe 2 O 4 ) catalyst with dual Lewis acid sites to realize the homolytic cleavage of H 2 O 2 . The results of systematic experiments, in situ characterizations, and theoretical calculations confirm that tetrahedral Cu sites with optimal Lewis acidity and strong electron delocalization can synergistically elongate the O−O bonds (1.47 Å → 1.87 Å) in collaboration with adjacent bridging hydroxyl (another Lewis acid site). As a result, the free energy of H 2 O 2 homolytic cleavage is…

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115
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Authors

6

Topics & keywords

Keywords
  • Homolysis
  • Lewis acids and bases
  • Catalysis
  • Chemistry
  • Bond cleavage
  • Hydroxyl radical
  • Cleavage (geology)
  • Delocalized electron
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