articleNature CommunicationsMar 6, 2024GOLD OA

In situ electrochemical regeneration of nanogap hotspots for continuously reusable ultrathin SERS sensors

University of Cambridge · Kangwon National University

PubMed
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Abstract

Abstract Surface-enhanced Raman spectroscopy (SERS) harnesses the confinement of light into metallic nanoscale hotspots to achieve highly sensitive label-free molecular detection that can be applied for a broad range of sensing applications. However, challenges related to irreversible analyte binding, substrate reproducibility, fouling, and degradation hinder its widespread adoption. Here we show how in-situ electrochemical regeneration can rapidly and precisely reform the nanogap hotspots to enable the continuous reuse of gold nanoparticle monolayers for SERS. Applying an oxidising potential of +1.5 V (vs Ag/AgCl) for 10 s strips a broad range of adsorbates from the nanogaps and forms a metastable oxide layer…

Citation impact

110
total citations
FWCI
11.90
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100%
References
70
Citations per year

Authors

9

Topics & keywords

Keywords
  • Materials science
  • Nanotechnology
  • Surface-enhanced Raman spectroscopy
  • Plasmon
  • In situ
  • Raman spectroscopy
  • Analyte
  • Nanoscopic scale
UN Sustainable Development Goals
  • Life in Land
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