articleJournal of the American Chemical SocietyMar 20, 2024Closed access

Enhancing H 2 O 2 Electrosynthesis at Industrial-Relevant Current in Acidic Media on Diatomic Cobalt Sites

State Key Laboratory of Chemical Engineering · Tsinghua University · +1 more institution

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Abstract

Electrocatalytic synthesis of hydrogen peroxide (H2O2) in acidic media is an efficient and eco-friendly approach to produce inherently stable H2O2, but limited by the lack of selective and stable catalysts under industrial-relevant current densities. Herein, we report a diatomic cobalt catalyst for two-electron oxygen reduction to efficiently produce H2O2 at 50–400 mA cm–2 in acid. Electrode kinetics study shows a >95% selectivity for two-electron oxygen reduction on the diatomic cobalt sites. In a flow cell device, a record-high production rate of 11.72 mol gcat–1 h–1 and exceptional long-term stability (100 h) are realized under high current densities. In situ spectroscopic studies and theoretical…

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