articleAdvanced MaterialsMar 22, 2024BRONZE OA

Sub‐2 nm IrRuNiMoCo High‐Entropy Alloy with Iridium‐Rich Medium‐Entropy Oxide Shell to Boost Acidic Oxygen Evolution

Shanghai Advanced Research Institute · University of Chinese Academy of Sciences · +1 more institution

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Abstract

Abstract Ensuring high catalytic activity and durability at low iridium (Ir)usage is still a big challenge for the development of electrocatalysts toward oxygen evolution reaction (OER) in proton exchange membrane water electrolysis (PEMWE). Here, a rapid liquid‐reduction combined with surface galvanic replacement strategy is reported to synthesize the sub 2 nm high‐entropy alloy (HEA) nanoparticles featured with Ir‐rich IrRuNiMo medium‐entropy oxide shell (Ir‐MEO) and a IrRuCoNiMo HEA core (HEA@Ir‐MEO). Advanced spectroscopies reveal that the Ir‐rich MEO shell inhibits the severe structural evolution of transition metals upon the OER, thus guaranteeing the structural stability. In situ differential…

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