articleAdvanced MaterialsApr 2, 2024Closed access

Efficient Electrochemical Co‐Reduction of Carbon Dioxide and Nitrate to Urea with High Faradaic Efficiency on Cobalt‐Based Dual‐Sites

University of Electronic Science and Technology of China · Sichuan University · +6 more institutions

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Abstract

Abstract Renewable electricity‐powered nitrate/carbon dioxide co‐reduction reaction toward urea production paves an attractive alternative to industrial urea processes and offers a clean on‐site approach to closing the global nitrogen cycle. However, its large‐scale implantation is severely impeded by challenging C–N coupling and requires electrocatalysts with high activity/selectivity. Here, cobalt‐nanoparticles anchored on carbon nanosheet (Co NPs@C) are proposed as a catalyst electrode to boost yield and Faradaic efficiency (FE) toward urea electrosynthesis with enhanced C–N coupling. Such Co NPs@C renders superb urea‐producing activity with a high FE reaching 54.3% and a urea yield of 2217.5 µg h −1 mg…

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