articleACS CatalysisApr 25, 2024Closed access

S-Scheme Heterojunction/Single-Atom Dual-Driven Charge Transport for Photocatalytic Hydrogen Production

National Center for Nanoscience and Technology · University of Chinese Academy of Sciences · +5 more institutions

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Abstract

The rational design and modification of heterojunction photocatalysts aimed at achieving fast charge transport and efficient photocatalytic performance is a central goal of solar-light-driven water splitting and hydrogen evolution, yet this remains a challenge. Herein, we prepare a hierarchical photocatalyst composed of a few-layer violet phosphorene (VP), cadmium sulfide (CdS) nanoparticles (NPs), and Pd single atoms (SAs) by a facile one-step ball-milling strategy. The underlying VP/CdS p–n heterojunctions are verified to adopt S-scheme directional charge transfer by combining in situ irradiated X-ray photoelectron spectroscopy and electron paramagnetic resonance. The atomically dispersed Pd sites of the…

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