articleAdvanced MaterialsJun 14, 2024BRONZE OA

Urea Electrosynthesis from Nitrate and CO 2 on Diatomic Alloys

Lanzhou Jiaotong University · Kunming University of Science and Technology · +2 more institutions

PubMed
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Abstract

Abstract Urea electrosynthesis from co–electrolysis of NO 3 − and CO 2 (UENC) offers a promising technology for achieving sustainable and efficient urea production. Herein, a diatomic alloy catalyst (CuPd 1 Rh 1 –DAA), with mutually isolated Pd and Rh atoms alloyed on Cu substrate, is theoretically designed and experimentally confirmed to be a highly active and selective UENC catalyst. Combining theoretical computations and operando spectroscopic characterizations reveals the synergistic effect of Pd 1 –Cu and Rh 1 –Cu active sites to promote the UENC via a tandem catalysis mechanism, where Pd 1 –Cu site triggers the early C–N coupling and promotes *CO 2 NO 2 –to–*CO 2 NH steps, while Rh 1 –Cu site facilitates…

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262
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Authors

10

Topics & keywords

Keywords
  • Catalysis
  • Electrosynthesis
  • Urea
  • Materials science
  • Inorganic chemistry
  • Yield (engineering)
  • Electrolysis
  • Faraday efficiency
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