articleJournal of the American Chemical SocietySep 5, 2024Closed access

Urea Synthesis via Coelectrolysis of CO 2 and Nitrate over Heterostructured Cu–Bi Catalysts

Chinese Academy of Sciences · Beijing National Laboratory for Molecular Sciences · +5 more institutions

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Abstract

Electrocatalytic coupling of CO2 and NO3– to urea is a promising way to mitigate greenhouse gas emissions, reduce waste from industrial processes, and store renewable energy. However, the poor selectivity and activity limit its application due to the multistep process involving diverse reactants and reactions. Herein, we report the first work to design heterostructured Cu–Bi bimetallic catalysts for urea electrosynthesis. A high urea Faradaic efficiency (FE) of 23.5% with a production rate of 2180.3 μg h–1 mgcat–1 was achieved in H-cells, which surpassed most reported electrocatalysts in the literature. Moreover, the catalyst had a remarkable recycling stability. Experiments and density functional theory…

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