articleJournal of the American Chemical SocietyJan 11, 2025Closed access

Catalyst-Free Nitrogen Fixation by Microdroplets through a Radical-Mediated Disproportionation Mechanism under Ambient Conditions

Xiamen University · Collaborative Innovation Center of Chemistry for Energy Materials · +6 more institutions

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Abstract

Nitrogen fixation is essential for the sustainable development of both human society and the environment. Due to the chemical inertness of the N≡N bond, the traditional Haber–Bosch process operates under extreme conditions, making nitrogen fixation under ambient conditions highly desirable but challenging. In this study, we present an ultrasonic atomizing microdroplet method that achieves nitrogen fixation using water and air under ambient conditions in a rationally designed sealed device, without the need for any catalyst. The total nitrogen fixation rate achieved is 6.99 μmol/h, yielding ammonium as the reduction product and nitrite and nitrate as the oxidation products, with hydrogen peroxide produced as a…

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