articleAngewandte Chemie International EditionJan 24, 2025Closed access

Tuning the Acid Hardness Nature of Cu Catalyst for Selective Nitrate‐to‐Ammonia Electroreduction

Chinese Academy of Sciences · Beijing National Laboratory for Molecular Sciences · +2 more institutions

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Abstract

Abstract Electrocatalytic nitrate reduction reaction (NO 3 RR) in alkaline electrolyte presents a sustainable pathway for energy storage and green ammonia (NH 3 ) synthesis. However, it remains challenging to obtain high activity and selectivity due to the limited protonation and/or desorption processes of key intermediates. Herein, we propose a strategy to regulate the acid hardness nature of Cu catalyst by introducing appropriate modifier. Using density functional theory calculations, we firstly identified that the BaO‐modified Cu showed optimal Gibbs free energies for key NO 3 RR steps, including the protonation of *NO and the desorption of *NH 3 . Experimentally, the BaO‐modified Cu catalyst exhibited 97.3…

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