articleChemistry of MaterialsMar 3, 2025Closed access

Confined Palladium Nanocrystals within Covalent Organic Framework-Intercalated MXene Nanoarchitectures toward Highly Efficient Methanol Electrooxidation

Hohai University · Division of Materials Science and Engineering · +2 more institutions

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Abstract

The rational design of high-performance electrocatalysts toward the methanol oxidation reaction plays a noticeable role in the progress of stimulating the industrial development of direct methanol fuel cells. In this study, ultrafine palladium nanocrystals are in situ confined within the hydrazone-linked covalent organic framework (COF-42)-intercalated Ti3C2Tx MXene nanoarchitectures (Pd/COF-MX) through a facile and robust stereoconstruction strategy. The existence of hydrangea-shaped COF-42 with abundant N species makes it possible to optimize the coordination environments for Pd nanocrystals to facilitate their size confinement and homogeneous dispersion, while the MXene nanosheets afford strong electronic…

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