articleACS Energy LettersApr 4, 2025Closed access

Boosting Oxygen Evolution Reaction Performance on BiVO 4 Photoanode via Gradient Oxygen Vacancies

Wuhan National Laboratory for Optoelectronics · Huazhong University of Science and Technology

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Abstract

BiVO4 is extensively studied in photoelectrochemical water splitting systems. Its relatively large bandgap and low charge carrier mobility severely limit the solar-driven oxygen evolution reaction on BiVO4. A gradient distribution of oxygen vacancies can modulate the structural and electrical properties of BiVO4. However, the formation of oxygen vacancies remains a daunting challenge. Here, we propose a simple hydrothermal post-treatment method to deposit a thin amorphous BiOx layer (∼8 nm) with gradient oxygen vacancies on the surface of BiVO4 and enable directional hole migration. The resultant BiVO4/BiOx/NiFeOx photoanode achieves a high photocurrent density of 6.34 mA cm–2 at 1.23 V (vs RHE) in 1.0 M…

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