articleAngewandte Chemie International EditionMay 5, 2025BRONZE OA

Interfacial Water Structure Modulation on Unconventional Phase Non‐Precious Metal Alloy Nanostructures for Efficient Nitrate Electroreduction to Ammonia in Neutral Media

City University of Hong Kong · Applied Science and Technology Research Institute · +15 more institutions

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Abstract

Abstract Electrocatalytic nitrate reduction reaction (NO 3 RR) has been recognized as a sustainable route for nitrate removal and value‐added ammonia (NH 3 ) synthesis. Regulating the surface active hydrogen (*H) behavior is crucial but remains a formidable challenge, especially in neutral electrolytes, greatly limiting the highly selective NH 3 formation. Herein, we report the controlled synthesis of heterophase hcp/fcc non‐precious CuNi alloy nanostructures for efficient NH 3 electrosynthesis in neutral media. Significantly, hcp/fcc Cu 10 Ni 90 exhibits excellent performance with NH 3 Faradaic efficiency and yield rate of 98.1% and 57.4 mg h −1 mg cat −1 , respectively. In situ studies suggest that the high…

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