articleAngewandte Chemie International EditionMay 19, 2025Closed access

Kelvin Probe Force Microscopy Reveals Spatially Resolved Charge‐Transfer Mechanism in CdS/BiOBr S‐scheme Heterojunction Photocatalyst

China University of Geosciences · China University of Geosciences (Beijing) · +2 more institutions

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Abstract

Abstract S‐scheme heterojunctions hold great promise for photocatalysis, yet a comprehensive understanding of their charge‐transfer mechanisms remains limited. While time‐resolved techniques have provided valuable insights, the spatial resolution of charge transfer at the material surface remains underexplored. Here, we employ Kelvin probe force microscopy (KPFM) to investigate the charge‐transfer dynamics in S‐scheme heterojunctions, revealing spatially resolved details. Our findings show that upon illumination, the Fermi level ( E f ) of n‐type semiconductors increases, but a built‐in electric field (IEF) persists within the heterojunction. Electrons accumulate on the surface of the reduction semiconductor…

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