articleJournal of the American Chemical SocietyJun 20, 2025HYBRID OA

Tiara Ni Clusters for Electrocatalytic Nitrate Reduction to Ammonia with 97% Faradaic Efficiency

Dalian Institute of Chemical Physics · Chinese Academy of Sciences · +3 more institutions

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Abstract

The electroreduction of nitrate (NO3–) for sustainable ammonia (NH3) production has recently emerged as a green process to solve water contamination and produce valuable chemicals. In this study, we developed Ni6@CuFe-LDH composites comprising tiara Ni6(SC2H4COOH)12 (Ni6) clusters anchored on the edges of 2D CuFe-LDH (LDH: layered double hydroxides) nanosheets via electrostatic interactions. The Ni6@CuFe-LDH catalyst exhibits high electrochemical performance in nitrate reduction reaction (NO3RR). Specifically, the Ni6@CuFe-LDH gives rise to an excellent faradaic efficiency of ∼97%, significantly surpassing the ∼73% FE of the pristine CuFe-LDH, with the NH3 productivity (0.91 mmol mg–1 h–1) being similar to…

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