articleEnvironmental Science & TechnologyJan 5, 2026Closed access

Multisite (Cu 0 /Cu + /Cu 2+ –Fe) Interfaces Enhance Nitrate Adsorption and Active Hydrogen Utilization for Ammonia Electrosynthesis from Neutral Nitrate

DLDanping LiTWTongde WangGGGuohua GaoHWHan WangLNLingfeng Ni

Tongji University · State Key Laboratory of Pollution Control and Resource Reuse · +2 more institutions

PubMed
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Abstract

The electroreduction of hazardous nitrate (NO3–) to valuable ammonia (NH3) represents a sustainable approach to environmental remediation and nitrogen recovery. However, most catalysts exhibit undesirable NH3 yield rates and poor Faradaic efficiency (FE) for the NO3– reduction reaction (NO3RR) in near-neutral and low-concentration NO3–environments. Herein, the Fe-doped multivalent copper oxide (CuxO–Fe) was prepared to construct multisite interfaces that promote NO3– adsorption and H2O dissociation-protonation processes. The CuxO–Fe catalyst achieves a superior NH3 yield rate of 3.5 mg·h–1·mgcat–1 (3.9 mg·h–1·cm–2), an excellent FE of 97.7%, and a NH3 selectivity of 98.7%, outperforming Fe oxide…

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