articleAngewandte Chemie International EditionJan 16, 2026Closed access

Pulse‐Electrodeposited Single‐Atom Alloys with Steered Surface Hydrogenation Dynamics for Air‐to‐Fertilizer Synthesis

University of Electronic Science and Technology of China · The University of Texas at Austin · +1 more institution

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Abstract

Abstract Harnessing renewable electricity to transform abundant environmental resources into fertilizers is central to sustainable development. Electrochemical nitrate‐to‐ammonia conversion provides a promising route, yet its efficiency is constrained by the elusive surface hydrogenation dynamics governing multi‐step *NO x reduction. Here, a cooperative descriptor (Ψ) derived from large‐language‐models‐assisted mining and energetic analysis successfully identifies NiCu single‐atom alloys (SAAs) as optimal catalysts. Pulse electrodeposition delivers atomically dispersed alloys with tunable structures, achieving a maximum Faradaic efficiency (FE) of ∼95% and yield rate (YR) of ∼11.4 mg h −1 cm −2 . In situ…

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6
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25.36
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100%
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38
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8

Topics & keywords

Keywords
  • Yield (engineering)
  • Electrochemistry
  • Renewable energy
  • Electrochemical energy conversion
  • Catalysis
  • Hydrogen
  • Faraday efficiency
  • Surface (topology)
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