articleEnergy & Environmental ScienceJan 1, 2026HYBRID OA

Unveiling the mechanism of lithium-mediated nitrogen reduction via operando X-ray scattering in a flow cell with hydrogen oxidation

NHNiklas H. DeisslerJBJ. Bjarke V. MygindVAValerie A. NiemannJBJakob B. PedersenVVValentin Vinci

Technical University of Denmark · SLAC National Accelerator Laboratory · +2 more institutions

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Abstract

Operando GI WAXS in a flow cell with HOR revealed LiNH 2 as the only stable crystalline intermediate in the lithium mediated nitrogen reduction reaction (Li-NRR) and the unique solid electrolyte interphase (SEI) formed by diglyme electrolytes.

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Topics & keywords

Topics
Keywords
  • Diglyme
  • Interphase
  • Electrolyte
  • Reduction (mathematics)
  • Lithium (medication)
  • Hydrogen
  • Nitrogen
  • Redox
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